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气相色谱法分析辽细辛中甲基丁香酚和黄樟醚的季节变化

[Analysis of season variation of methyleugenol and safrole in Asarum heterotropoides by gas chromatography].

作者信息

Wang D, Wang X, Xia X

机构信息

Heilongjiang University of Traditional Chinese Medicine, Harbin, 150040.

出版信息

Se Pu. 1997 Jan;15(1):85-6.

Abstract

We established a method for quantitative analysis of methyleugenol and safrole in Asarum heterotropoides by GC to study their season variation. The results showed that the content of methyleugenol in the essential oil of the subterranean part of different seasons was 21%-39%, and that for safrole was 17%-33%. In the upterranean part, methyleugenol was 1.4%-9.6%, and safrole was 0.36%-2.1%. It is clear that methyleugenol and safrole are provided mainly by the subterranean part. The quantity of methyleugenol is the richest in the period of sprouting and after-fruiting, and for the safrole content the richest periods are that of sprouting, blooming and after-fruiting. In the case of upterranean part, the richest time is blooming period both for methyleugenol and safrole, and after blooming they decrease gradually.

摘要

我们建立了一种用气相色谱法对北细辛中甲基丁香酚和黄樟醚进行定量分析的方法,以研究它们的季节变化。结果表明,不同季节地下部分精油中甲基丁香酚的含量为21%-39%,黄樟醚的含量为17%-33%。地上部分中,甲基丁香酚为1.4%-9.6%,黄樟醚为0.36%-2.1%。显然,甲基丁香酚和黄樟醚主要由地下部分提供。甲基丁香酚的含量在发芽期和结果后期最为丰富,而黄樟醚含量最丰富的时期是发芽期、开花期和结果后期。对于地上部分,甲基丁香酚和黄樟醚含量最丰富的时间都是开花期,开花后它们逐渐减少。

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