Sundh Anders, Molin Margareta, Sjögren Göran
Department of Odontology, Faculty of Medicine, Umeå University, SE-901 87 Umeå, Sweden.
Dent Mater. 2005 May;21(5):476-82. doi: 10.1016/j.dental.2004.07.013. Epub 2004 Dec 2.
Yttria-stabilized zirconia (Y-TZP) ceramic is a high-performance material with excellent mechanical properties suitable for fixed partial dentures. The purpose of this study was to evaluate after fatigue testing, the effect of heat-treatment and veneering on the fracture resistance of frameworks manufactured using sintered and subsequently hot isostatic pressed yttrium oxide partially-stabilized zirconia (Denzir).
The specimens were subjected to dynamic loading in water. Thereafter, using a universal testing machine, the fracture resistance of three-unit fixed partial dentures was determined; (i) of the frameworks as delivered after machining, (ii) after the frameworks had been subjected to heat-treatment similar to veneering with a glass-ceramic (Eris) or a feldspar-based ceramic (Vita D) and (iii) after the frameworks had been veneered with these ceramics. In addition, the fracture resistance of frameworks as delivered after machining not subjected to dynamic loading in water was determined.
Cyclic loading in water did not significantly (p>0.05) affect the fracture resistance. The load necessary to fracture the frameworks as delivered after machining was significantly (p<0.001) higher than for the heat-treated and veneered specimens. No significant difference was seen between the specimens veneered with Eris and those veneered with Vita D (p>0.05). For all but three specimens the fractures were located in the loading point and through one of the connectors.
Heat-treatment and veneering reduce fracture resistance of hot isostatic pressed zirconia. Nevertheless, the results obtained indicate that it is an interesting material for potential in all-ceramic restorations.
钇稳定氧化锆(Y-TZP)陶瓷是一种具有优异机械性能的高性能材料,适用于固定局部义齿。本研究的目的是评估疲劳测试后,热处理和 veneering 对使用烧结并随后进行热等静压的氧化钇部分稳定氧化锆(Denzir)制造的框架的抗断裂性的影响。
将标本在水中进行动态加载。此后,使用万能试验机测定三单位固定局部义齿的抗断裂性;(i)加工后交付的框架的抗断裂性,(ii)框架经过类似于用玻璃陶瓷(Eris)或长石基陶瓷(Vita D)进行 veneering 的热处理后的抗断裂性,以及(iii)框架用这些陶瓷进行 veneering 后的抗断裂性。此外,还测定了加工后交付的未在水中进行动态加载的框架的抗断裂性。
水中的循环加载对抗断裂性没有显著(p>0.05)影响。加工后交付的框架断裂所需的载荷显著(p<0.001)高于热处理和 veneered 标本。用 Eris veneered 的标本和用 Vita D veneered 的标本之间没有显著差异(p>0.05)。除三个标本外,所有标本的骨折都位于加载点并穿过其中一个连接器。
热处理和 veneering 会降低热等静压氧化锆的抗断裂性。然而,获得的结果表明它是一种用于全陶瓷修复体的潜在有趣材料。