Nagai T, Kawamoto Y, Kakehashi Y, Matsumura H
Department of Crown and Bridge Prosthodontics, Nihon University School of Dentistry, 1-8-13 Kanda-Surugadai, Chiyoda-ku, Tokyo 101-8310, Japan.
J Oral Rehabil. 2005 Aug;32(8):598-605. doi: 10.1111/j.1365-2842.2005.01464.x.
This study evaluates the bonding characteristics of a lithium disilicate-based ceramic material (IPS Empress 2). Two sizes of disk specimens of the material were made, and three groups of disk pairs were separately surface-prepared using three techniques; etching with phosphoric acid, etching with hydrofluoric acid, and air-abrasion with alumina. Each group was further divided into four sub-groups; group (i) was bonded with the Variolink II composite, (ii) was treated with the Monobond-S silane primer and bonded with the Variolink II composite, (iii) was bonded with the Super-Bond acrylic adhesive and (iv) was treated with the Porcelain Liner M silane primer and bonded with the Super-Bond acrylic adhesive. Shear bond strengths were determined before and after 100 000 thermocycles. Bond strength varied from 10.6 to 71.5 MPa before thermocycling, whereas post-thermocycling bond strength ranged from 0 to 61.2 MPa. Among the three surface preparations, hydrofluoric acid etching (HF) was most effective in enhancing bond strength of both luting materials, especially for unsilanized specimens. Application of the silane primer elevated bond strength of both luting agents regardless of surface preparation method. It can be concluded, for both luting agents, that durable bond to the Empress 2 ceramic material can be achieved through the combined application of HF and the proprietary silane primer.
本研究评估了一种基于二硅酸锂的陶瓷材料(IPS Empress 2)的粘结特性。制作了该材料的两种尺寸的圆盘试样,并使用三种技术分别对三组圆盘对进行表面处理;用磷酸蚀刻、用氢氟酸蚀刻以及用氧化铝进行空气研磨。每组进一步分为四个亚组;第(i)组用Variolink II复合材料粘结,(ii)组用Monobond - S硅烷底漆处理后再用Variolink II复合材料粘结,(iii)组用Super - Bond丙烯酸粘合剂粘结,(iv)组用Porcelain Liner M硅烷底漆处理后再用Super - Bond丙烯酸粘合剂粘结。在100000次热循环前后测定剪切粘结强度。热循环前粘结强度在10.6至71.5MPa之间变化,而热循环后粘结强度范围为0至61.2MPa。在三种表面处理方法中,氢氟酸蚀刻(HF)在提高两种粘结材料的粘结强度方面最为有效,尤其是对于未用硅烷处理的试样。无论表面处理方法如何,硅烷底漆的应用都提高了两种粘结剂的粘结强度。对于两种粘结剂都可以得出结论,通过联合应用HF和专利硅烷底漆,可以实现与Empress 2陶瓷材料的持久粘结。