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Comparison of silanization/hydrosilation and organosilanization modification procedures on etched capillaries for electrokinetic chromatography.

作者信息

Matyska Maria T, Pesek Joseph J

机构信息

Department of Chemistry, San Jose State University, One Washington Square, San Jose, CA 95192, USA.

出版信息

J Chromatogr A. 2005 Jun 24;1079(1-2):366-71. doi: 10.1016/j.chroma.2005.03.010.

DOI:10.1016/j.chroma.2005.03.010
PMID:16038324
Abstract

Etched capillaries for use in open tubular electrochromatography are modified by silanization/hydrosilation and organosilanization. The migration behavior of both types of capillaries is evaluated with small basic molecules, peptides and proteins. Comparisons of peak symmetry and efficiency are used to measure the effectiveness of the two methods for modifying the etched surface. From this information, the suitability of each method for use with etched capillaries can be determined.

摘要

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