Lenk Andreas, Lichte Hannes, Muehle Uwe
Institute of Structure Physics, Dresden University, D-01062 Dresden, Germany.
J Electron Microsc (Tokyo). 2005 Aug;54(4):351-9. doi: 10.1093/jmicro/dfi055. Epub 2005 Aug 25.
Transmission electron microscopy (TEM) is a widely used tool for analysis of very large scale integrated (VLSI) semiconductor devices. As a special TEM-feature, off-axis electron holography obtains information about the electrical characteristics of a specimen, which are connected to the dopant concentration in the bulk material. Compared with conventional TEM, application of electron holography for dopant profiling demands a higher quality of specimen preparation, e.g. in terms of thickness homogeneity. Since preparation by means of focused ion beam (FIB) has become an industrial standard for TEM-investigations, its facilities are investigated for meeting the high holographic demands. It turned out that, besides many advantages like precision and speed, the use of FIB for preparation introduces new specific problems, e.g. it is hardly possible to visualize doped areas of semiconductors on a classical, thin FIB specimen. Additionally, some artifacts of FIB-preparation have no great importance for normal TEM analysis, but do significantly influence the results of holographic analysis. In order to satisfy the higher demands of preparation for holography, a special procedure for FIB-preparation has been newly developed.
透射电子显微镜(TEM)是一种广泛用于分析超大规模集成(VLSI)半导体器件的工具。作为TEM的一项特殊功能,离轴电子全息术可获取与样品电学特性相关的信息,而这些特性与块状材料中的掺杂剂浓度有关。与传统TEM相比,将电子全息术用于掺杂剂剖析需要更高质量的样品制备,例如在厚度均匀性方面。由于借助聚焦离子束(FIB)进行制备已成为TEM研究的行业标准,因此对其设备进行了研究以满足全息术的高要求。结果表明,除了精度和速度等诸多优点外,使用FIB进行制备还会带来新的特定问题,例如在经典的薄FIB样品上几乎无法观察到半导体的掺杂区域。此外,FIB制备的一些伪像对常规TEM分析影响不大,但会显著影响全息分析的结果。为了满足全息术制备的更高要求,新开发了一种特殊的FIB制备程序。