Hüe F, Johnson C L, Lartigue-Korinek S, Wang G, Buseck P R, Hÿtch M J
CECM-CNRS, 15 rue Georges Urbain, 94407 Vitry-sur-Seine, France.
J Electron Microsc (Tokyo). 2005 Jun;54(3):181-90. doi: 10.1093/jmicro/dfi042. Epub 2005 Aug 25.
The distortions introduced into high-resolution transmission electron microscope (HRTEM) images by the projector lens system are an important source of systematic error for quantitative displacement and strain determination. Using geometric phase analysis of images of perfect crystals, we measured these errors for two different transmission electron microscopes. Local magnification varies by as much as 5%, and rotation can reach 2 degrees across a typical image. Our experimental results are compared with theory, and optical pincushion and spiral distortion coefficients are determined. A method for calibrating and removing these distortions is presented that enables quantification to 0.1% strain and 0.1 degrees rotation across the whole field of view. This calibration is also critical for the accurate measurement of local lattice parameters from HRTEM images.
投影透镜系统引入高分辨率透射电子显微镜(HRTEM)图像中的畸变是定量位移和应变测定中系统误差的一个重要来源。通过对完美晶体图像进行几何相位分析,我们测量了两种不同透射电子显微镜的这些误差。局部放大率变化高达5%,在典型图像中旋转可达2度。我们将实验结果与理论进行了比较,并确定了光学枕形畸变和螺旋畸变系数。提出了一种校准和消除这些畸变的方法,该方法能够在整个视场范围内将应变量化到0.1%,旋转量化到0.1度。这种校准对于从HRTEM图像准确测量局部晶格参数也至关重要。