Maehara Satoshi, Fujishima Akihiro, Hotta Yasuhiro, Miyazaki Takashi
Department of Oral Biomaterials and Technology, Showa University School of Dentistry, 1-5-8 Hatanodai, Shinagawa-ku, Tokyo 142-8555, Japan.
Dent Mater J. 2005 Sep;24(3):328-34. doi: 10.4012/dmj.24.328.
This study examined fracture toughness (KIC) measurements obtained using the indentation fracture (IF) method with a view to improving their reliability. The KIC values of five dental ceramics were measured using the IF method with five different formulas, and the single-edge precracked beam (SEPB) method was used as a control. The elastic moduli of the dental ceramics were evaluated by dynamic hardness test. Load conditions of the dental ceramics that produced a median/radial crack for the IF method formulas were investigated. Based on the resultant c/a and P/c1.5 values, the indentation load (P) required for median/radial crack occurrence varied greatly from 29.4 to 196 N depending on the ceramic used. Among the five formulas, none of the KIC values obtained by the IF method with Miyoshi's formula differed significantly (p > 0.05) from the values obtained using SEPB method. These results suggested that, after an appropriate indentation load is determined, reliable KIC values for small dental ceramic specimens can be easily obtained using the IF method if Miyoshi's formula is used in combination with the dynamic hardness test.
本研究对采用压痕断裂(IF)法获得的断裂韧性(KIC)测量结果进行了检验,旨在提高其可靠性。使用IF法和五种不同公式测量了五种牙科陶瓷的KIC值,并采用单边预裂纹梁(SEPB)法作为对照。通过动态硬度测试评估牙科陶瓷的弹性模量。研究了IF法公式产生中位/径向裂纹的牙科陶瓷的载荷条件。根据所得的c/a和P/c1.5值,中位/径向裂纹出现所需的压痕载荷(P)根据所用陶瓷的不同,在29.4至196 N之间有很大差异。在这五个公式中,使用三吉公式的IF法获得的KIC值与使用SEPB法获得的值相比,均无显著差异(p>0.05)。这些结果表明,在确定合适的压痕载荷后,如果将三吉公式与动态硬度测试结合使用,使用IF法可以轻松获得小型牙科陶瓷试样可靠的KIC值。