Taira M, Nomura Y, Wakasa K, Yamaki M, Matsui A
Department of Dental Materials, School of Dentistry, Hiroshima University, Japan.
J Oral Rehabil. 1990 Nov;17(6):551-63. doi: 10.1111/j.1365-2842.1990.tb01426.x.
One important mechanical property of dental ceramics is fracture toughness, KIC, which represents the serviceability in the oral cavity, such as the resistance to marginal fracture. KIC values of several dental ceramics, natural tooth enamel and industrial ceramics were examined by use of the indentation microfracture (IM) method. This technique was based on the series of radial cracks emanating from the corners of the Vickers indentation. It was observed that appropriate load levels should be selected on each specimen to induce radial/median cracks. For feldspatic dental porcelains, larger loads of 10, 20 and 30 kg were needed to determine their KIC values in the range 1.5-2.1 MN.m-3/2. For natural tooth enamel and a new apatite-based castable glass-ceramic, a smaller force of 1 kg was sufficient to decide the respective KIC values of about 0.9 and 1.8 MN.m-3/2. The KIC values of most dental ceramics examined were slightly higher than that of soda lime glass, but less than one-third that of zirconia. It was confirmed that the IM method is simple and cost-effective for evaluation of KIC of dental ceramics.
牙科陶瓷的一个重要力学性能是断裂韧性KIC,它代表了在口腔中的适用性,比如对边缘断裂的抵抗能力。通过压痕微裂纹(IM)法检测了几种牙科陶瓷、天然牙釉质和工业陶瓷的KIC值。该技术基于从维氏压痕角发出的一系列径向裂纹。据观察,应在每个试样上选择合适的载荷水平以诱导径向/中位裂纹。对于长石质牙科瓷,需要10、20和30千克的较大载荷来确定其在1.5 - 2.1 MN.m-3/2范围内的KIC值。对于天然牙釉质和一种新型磷灰石基可铸微晶玻璃,1千克的较小力就足以确定各自约为0.9和1.8 MN.m-3/2的KIC值。所检测的大多数牙科陶瓷的KIC值略高于钠钙玻璃,但不到氧化锆的三分之一。证实了IM法对于评估牙科陶瓷的KIC简单且经济有效。