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The preparation of 3:5-dinitrobenzoic acid and 3:5-dinitrobenzoyl chloride: Observations on the acylation of amino-acids by means of 3:5-dinitrobenzoyl chloride and certain other acid chlorides.

作者信息

Saunders B C, Stacey G J, Wilding I G

机构信息

The University Chemical Laboratories, Cambridge.

出版信息

Biochem J. 1942 Apr;36(3-4):368-75. doi: 10.1042/bj0360368.

DOI:10.1042/bj0360368
PMID:16747534
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC1265703/
Abstract
摘要

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1
The preparation of 3:5-dinitrobenzoic acid and 3:5-dinitrobenzoyl chloride: Observations on the acylation of amino-acids by means of 3:5-dinitrobenzoyl chloride and certain other acid chlorides.3:5-二硝基苯甲酸和3:5-二硝基苯甲酰氯的制备：关于用3:5-二硝基苯甲酰氯及某些其他酰氯对氨基酸进行酰化反应的观察
Biochem J. 1942 Apr;36(3-4):368-75. doi: 10.1042/bj0360368.
2
A new method for the determination of serum creatinine based on reaction with 3.5-dinitrobenzoyl chloride in an organic medium.
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Determination of enantiomeric composition by negative-ion electrospray ionization-mass spectrometry using deprotonated N-(3,5-dinitrobenzoyl)amino acids as chiral selectors.以去质子化的N-（3,5-二硝基苯甲酰基）氨基酸为手性选择剂，通过负离子电喷雾电离质谱法测定对映体组成。
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Homogeneous acylation of xylan with 3,5-dinitrobenzoyl in ionic liquid and the adsorption property.在离子液体中用 3,5-二硝基苯甲酰均匀酰化木聚糖及其吸附性能。
Carbohydr Polym. 2015 Sep 5;128:105-11. doi: 10.1016/j.carbpol.2015.04.006. Epub 2015 Apr 15.
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The identification of amino-acids by means of 3:5-dinitrobenzoyl chloride.通过3:5-二硝基苯甲酰氯鉴定氨基酸。
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[Effectiveness of acylation of protein amino groups with fatty acid chlorides in a system of reversed micelles of aerosol OT in octane].
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Chiral separation on various modified amino alcohol-derived HPLC chiral stationary phases.在各种改性氨基醇衍生的高效液相色谱手性固定相上的手性分离。
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Solid-phase synthesis of chiral stationary phases based on 2,4,5,6-tetrachloro-1,3-dicyanobenzene derivatives spaced from N-3,5-dinitrobenzoyl alpha-amino acids: comparative study of their resolution efficacy.
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Unusual resolution of N-(3,5-dinitrobenzoyl)-alpha-amino acids on a chiral stationary phase based on (+)-(18-crown-6)-2,3,11,12-tetracarboxylic acid.基于（+）-（18-冠-6）-2,3,11,12-四羧酸的手性固定相上N-（3,5-二硝基苯甲酰基）-α-氨基酸的异常拆分
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HPLC analysis of polyamines and their acetylated derivatives in the picomole range using benzoyl chloride and 3,5-dinitrobenzoyl chloride as derivatizing agent.使用苯甲酰氯和3,5-二硝基苯甲酰氯作为衍生化试剂，对皮摩尔范围内的多胺及其乙酰化衍生物进行高效液相色谱分析。
Biomed Chromatogr. 1988 Nov;2(6):254-7. doi: 10.1002/bmc.1130020606.

引用本文的文献

1
3,5-Dinitro-benzoyl chloride.3,5-二硝基苯甲酰氯
Acta Crystallogr Sect E Struct Rep Online. 2009 Sep 12;65(Pt 10):o2460. doi: 10.1107/S1600536809036228.

本文引用的文献

1
The 3:5-dinitrobenzoyl derivatives of the amino-acids and their use in separating the isomers of leucine and valine.氨基酸的3,5-二硝基苯甲酰衍生物及其在分离亮氨酸和缬氨酸异构体中的应用。
Biochem J. 1941 Apr;35(4):578-87. doi: 10.1042/bj0350578.
2
Some applications of periodic acid to the study of the hydroxyamino-acids of protein hydrolysates: The liberation of acetaldehyde and higher aldehydes by periodic acid. 2. Detection and isolation of formaldehyde liberated by periodic acid. 3. Ammonia split from hydroxyamino-acids by periodic acid. 4. The hydroxyamino-acid fraction of wool. 5. ;Hydroxylysine' With an Appendix by Florence O. Bell Textile Physics Laboratory, University of Leeds.高碘酸在蛋白质水解产物中羟基氨基酸研究的一些应用：高碘酸使乙醛和高级醛的释放。2. 检测和分离高碘酸释放的甲醛。3. 高碘酸从羟基氨基酸中分解出的氨。4. 羊毛中的羟基氨基酸部分。5. “羟赖氨酸” 附佛罗伦萨·O·贝尔撰写的附录 利兹大学纺织物理实验室
Biochem J. 1941 Mar;35(3):294-314.1. doi: 10.1042/bj0350294.
3
The identification of amino-acids by means of 3:5-dinitrobenzoyl chloride.通过3:5-二硝基苯甲酰氯鉴定氨基酸。
Biochem J. 1934;28(2):580-6. doi: 10.1042/bj0280580.