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Nondestructive determination of arsenic in urine by epithermal neutron activation analysis and Compton suppression.

作者信息

Landsberger S, Swift G, Neuhoff J

机构信息

Department of Nuclear Engineering, University of Illinois, Urbana 61801.

出版信息

Biol Trace Elem Res. 1990 Jul-Dec;26-27:27-32. doi: 10.1007/BF02992655.

DOI:10.1007/BF02992655
PMID:1704729
Abstract

Epithermal neutron activation analysis, in conjunction with Compton suppression, has been employed to determine arsenic levels in artificially doped urine samples. Typical detection limits were of the order of 10 ng/g. Replicate determinations gave precision values between 2 and 12%, whereas accuracy measurements were between +/- 1 and +/- 20%. Biological and geological reference materials from the National Institute of Standards and Technology (NIST) were also analyzed for arsenic content. Typically, the precision achieved again was between 2 and 12%, whereas the accuracy measurements were in excellent agreement with the certified values.

摘要

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本文引用的文献

1
Chromium, nickel, and arsenic determinations in human samples by thermal and epithermal neutron activation analyses.用热中子和超热中子激活分析测定人发中的铬、镍和砷。
Biol Trace Elem Res. 1987 Aug;13(1):357-62. doi: 10.1007/BF02796646.
2
Reference values for the concentrations of As, Cd, Co, Cr, Cu, Fe, I, Hg, Mn, Mo, Ni, Pb, Se, and Zn in selected human tissues and body fluids.某些人体组织和体液中砷、镉、钴、铬、铜、铁、碘、汞、锰、钼、镍、铅、硒和锌浓度的参考值。
Biol Trace Elem Res. 1987 Apr;12(1):263-95. doi: 10.1007/BF02796686.
3
Comparison of several methods for the determination of arsenic compounds in water and in urine. Their application for the study of arsenic metabolism and for the monitoring of workers exposed to arsenic.
几种测定水和尿液中砷化合物方法的比较。它们在砷代谢研究及砷接触工人监测中的应用。
Int Arch Occup Environ Health. 1980;46(1):11-29. doi: 10.1007/BF00377456.
4
Neutron activation analysis for bulk and trace elements in urine.尿液中常量和微量元素的中子活化分析。
Anal Chim Acta. 1975 Sep;78(2):317-27. doi: 10.1016/S0003-2670(00)00152-5.
5
A nationwide survey of heavy metal absorption in children living near primary copper, lead, and zinc smelters.一项针对居住在初级铜、铅和锌冶炼厂附近儿童重金属吸收情况的全国性调查。
Am J Epidemiol. 1977 Oct;106(4):261-73. doi: 10.1093/oxfordjournals.aje.a112462.