Katritzky Alan R, Khashab Niveen M, Kirichenko Nataliya, Singh Anamika
Center for Heterocyclic Compounds, University of Florida, Department of Chemistry, Gainesville, Florida 32611-7200, USA.
J Org Chem. 2006 Nov 24;71(24):9051-6. doi: 10.1021/jo061410u.
In an operationally straightforward and efficient method, amidrazones and amidoximes are prepared in yields of 65-87% from imidoylbenzotriazoles by microwave heating for 5-20 min with the appropriate hydrazine or hydroxylamine.
采用一种操作简单且高效的方法,通过用适当的肼或羟胺对亚胺基苯并三唑进行5至20分钟的微波加热,可制备脒腙和偕胺肟,产率为65%至87%。