Walentek A, Seefeldt M, Verlinden B, Aernoudt E, Van Houtte P
Katholieke Universiteit Leuven, Department of Metallurgy and Materials Engineering (MTM), Kasteelpark Arenberg 44, B-3001 Heverlee, Belgium.
J Microsc. 2006 Dec;224(Pt 3):256-63. doi: 10.1111/j.1365-2818.2006.01702.x.
Electron backscatter diffraction measurements were performed on a set of pearlitic steel samples after different heat treatments. The strengths and limitations of the technique with respect to the pearlite issue are presented. Interpretation of the obtained results confirmed that more than one pearlite colony may exist inside one ferrite nodule of nearly the same crystallographic orientation. It was also found that, in most cases, a misorientation of the order of several degrees exists between pearlite colonies within one ferrite nodule. Moreover, the ferrite matrix exhibits changes of crystallographic orientation inside colonies often accompanied by a network of low angle boundaries. The mean size of the ferrite nodule in the matrix was determined by means of electron backscatter diffraction. However, determination of the mean pearlite colony size was difficult and often impossible by means of both metallographic methods and electron backscatter diffraction measurements.
对一组经过不同热处理的珠光体钢样品进行了电子背散射衍射测量。介绍了该技术在珠光体问题方面的优势和局限性。对所得结果的解释证实,在几乎相同晶体取向的一个铁素体晶粒内可能存在不止一个珠光体团。还发现,在大多数情况下,一个铁素体晶粒内的珠光体团之间存在几角度量级的取向差。此外,铁素体基体在晶团内部表现出晶体取向的变化,且常常伴有低角度晶界网络。通过电子背散射衍射确定了基体中铁素体晶粒的平均尺寸。然而,通过金相方法和电子背散射衍射测量来确定珠光体团的平均尺寸都很困难,而且常常无法做到。