Hemmerling C, Risto C, Augustyniak B, Jenner K
Bezirks-Hygiene-Institut Frankfurt(Oder), Bundesrepublik Deutschland.
Nahrung. 1991;35(7):711-9. doi: 10.1002/food.19910350711.
The treatment of water, soil and food samples was tested with a modified equipment of glass for simultaneous steam distillation/solvent extraction. Spiked samples with 22 pesticides (most of them contained halogen) and PCB yielded good or very good recoveries after 1.5 h for water samples and after 5 h for soil and plant food samples, respectively. This method is ecologically beneficial, and because it needs only a small amount of solvent (less than 10 ml) it is not expensive and may be used as a quick screening in several fields.
使用一种改良的玻璃设备对水、土壤和食品样品进行处理,以实现同时进行蒸汽蒸馏/溶剂萃取。添加了22种农药(其中大多数含有卤素)和多氯联苯的加标样品,水样在1.5小时后、土壤和植物性食品样品在5小时后分别获得了良好或非常好的回收率。该方法具有生态效益,并且由于仅需少量溶剂(少于10毫升),成本不高,可用于多个领域的快速筛查。