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[通过连续蒸汽蒸馏制备用于农药和多氯联苯残留分析的食品和环境样品]

[The preparation of food and environmental samples for residue analysis of pesticides and PCBs by continuous steam distillation].

作者信息

Hemmerling C, Risto C, Augustyniak B, Jenner K

机构信息

Bezirks-Hygiene-Institut Frankfurt(Oder), Bundesrepublik Deutschland.

出版信息

Nahrung. 1991;35(7):711-9. doi: 10.1002/food.19910350711.

DOI:10.1002/food.19910350711
PMID:1758476
Abstract

The treatment of water, soil and food samples was tested with a modified equipment of glass for simultaneous steam distillation/solvent extraction. Spiked samples with 22 pesticides (most of them contained halogen) and PCB yielded good or very good recoveries after 1.5 h for water samples and after 5 h for soil and plant food samples, respectively. This method is ecologically beneficial, and because it needs only a small amount of solvent (less than 10 ml) it is not expensive and may be used as a quick screening in several fields.

摘要

使用一种改良的玻璃设备对水、土壤和食品样品进行处理,以实现同时进行蒸汽蒸馏/溶剂萃取。添加了22种农药(其中大多数含有卤素)和多氯联苯的加标样品,水样在1.5小时后、土壤和植物性食品样品在5小时后分别获得了良好或非常好的回收率。该方法具有生态效益,并且由于仅需少量溶剂(少于10毫升),成本不高,可用于多个领域的快速筛查。

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