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[Separation of epimers of anisodamine (654-2) with HPLC using chiral additives in the mobile phase].

作者信息

Xie L, Chi H, Zhou T H

机构信息

Institute of Materia Medica, Chinese Academy of Medical Sciences, Beijing.

出版信息

Yao Xue Xue Bao. 1991;26(7):527-30.

PMID:1805511
Abstract

The separation of epimers of anisodamine were studied with HPLC using a reversed phase ODS C18 column. Several chiral additives were tried in the mobile phases. d-Camphorsulfonic acid and L-(+)-dibutyl tartrate showed good resolution ability for the separation of the isomers, a pair of epimers of anisodamine were well separated; while beta-cyclodextrin appeared to have no selectivity for the epimers.

摘要

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