Xie J X
Zhongguo Yi Xue Ke Xue Yuan Xue Bao. 1989 Dec;11(6):449-52.
A study on the quantitative-determination of a synthetic new drug--(+/-) anisodamine with HPLC is described. The analysis was completed on a stainless steel column (phi 4 X 250 mm) packed with a chemical bonded phase (YWG-C18H37), the mobile phase being a mixture of methanol, water and triethylamine (V/V/V 255:45:0.01) with a flow rate of 1 ml/min at room temperature. The (+/-)-anisodamine was detected by UV at 254 nm. This method is rapid, reproducible and accurate, and can be used for quantitative determination of (+/-) anisodamine in different product batches.