Geiger Dorin, Lichte Hannes, Linck Martin, Lehmann Michael
Institute for Structure Physics, Triebenberg Laboratory, Technische Universität Dresden, D-01062 Dresden, Germany.
Microsc Microanal. 2008 Feb;14(1):68-81. doi: 10.1017/S143192760808001X. Epub 2007 Dec 21.
Cs correctors have revolutionized transmission electron microscopy (TEM) in that they substantially improve point resolution and information limit. The object information is found sharply localized within 0.1 nm, and the intensity image can therefore be interpreted reliably on an atomic scale. However, for a conventional intensity image, the object exit wave can still not be detected completely in that the phase, and hence indispensable object information is missing. Therefore, for example, atomic electric-field distributions or magnetic domain structures cannot be accessed. Off-axis electron holography offers unique possibilities to recover completely the aberration-corrected object wave with uncorrected microscopes and hence we would not need a Cs-corrected microscope for improved lateral resolution. However, the performance of holography is affected by aberrations of the recording TEM in that the signal/noise properties ("phase detection limit") of the reconstructed wave are degraded. Therefore, we have realized off-axis electron holography with a Cs-corrected TEM. The phase detection limit improves by a factor of four. A further advantage is the possibility of fine-tuning the residual aberrations by a posteriori correction. Therefore, a combination of both methods, that is, Cs correction and off-axis electron holography, opens new perspectives for complete TEM analysis on an atomic scale.
球差校正器彻底改变了透射电子显微镜(TEM),因为它们极大地提高了点分辨率和信息极限。物体信息被精确地定位在0.1纳米范围内,因此强度图像可以在原子尺度上得到可靠的解释。然而,对于传统的强度图像,物体出射波仍然无法被完全检测到,因为相位以及因此而不可或缺的物体信息缺失了。因此,例如,原子电场分布或磁畴结构无法被获取。离轴电子全息术提供了独特的可能性,即使用未校正的显微镜完全恢复像差校正后的物体波,因此我们不需要使用球差校正显微镜来提高横向分辨率。然而,全息术的性能受到记录TEM的像差的影响,因为重建波的信号/噪声特性(“相位检测极限”)会降低。因此,我们实现了使用球差校正TEM的离轴电子全息术。相位检测极限提高了四倍。另一个优点是可以通过后验校正对残余像差进行微调。因此,这两种方法的结合,即球差校正和离轴电子全息术,为原子尺度上的完整TEM分析开辟了新的前景。