Polydorou Olga, Beiter Johannes, König Armin, Hellwig Elmar, Kümmerer Klaus
Department of Operative Dentistry and Periodontology, University Medical Center Freiburg, Dental School and Hospital, Hugstetter Strasse 55, 79106 Freiburg i. Br., Germany.
Dent Mater. 2009 Feb;25(2):254-60. doi: 10.1016/j.dental.2008.07.004. Epub 2008 Sep 7.
The aim of this study was to evaluate the effect of bleaching on the elution of monomers from two modern composite materials.
Two different resin composites (a nanohybrid the Filtek Supreme XT and an ormocer the Ceram X) were bleached with two products (hydrogen peroxide 38% for 45 min and carbamide peroxide 15% for 56 h). Four groups (n=10, diameter: 4.5 mm, thickness: 2 mm) of each material were fabricated, two for each bleaching product. One group was used as unbleached control and the other one was bleached. Then the samples were stored in 1 ml of 75 vol% ethanol at room temperature, and the storage medium was renewed after 24 h, 7 days, and 28 days. From the storage medium that was removed samples were prepared and analysed with LC-MS/MS.
None of the bleaching products had an effect on the amount of Bis-GMA and TEGDMA released from Ceram X. The amount of Bisphenol A released from the bleached samples of Ceram X was significantly lower compared to the control samples. Bleaching reduced significantly the amount of Bis-GMA released from Filtek Supreme XT. The amount of TEGDMA released from Filtek Supreme XT was not affected by bleaching.
The bleaching agents tested in the present study reduced the amount of some of the monomers released from the two composite materials. Bleaching of modern composite materials does not increase the release of monomers.
本研究旨在评估漂白对两种现代复合材料中单体洗脱的影响。
两种不同的树脂复合材料(纳米混合材料Filtek Supreme XT和有机陶瓷材料Ceram X)用两种产品进行漂白(38%过氧化氢45分钟和15%过氧化脲56小时)。每种材料制备四组(n = 10,直径:4.5毫米,厚度:2毫米),每种漂白产品两组。一组用作未漂白对照,另一组进行漂白。然后将样品在室温下保存在1毫升75%体积分数的乙醇中,24小时、7天和28天后更换储存介质。从取出的储存介质中制备样品并用液相色谱-串联质谱法(LC-MS/MS)进行分析。
两种漂白产品对从Ceram X中释放的双酚A缩水甘油醚(Bis-GMA)和三乙二醇二甲基丙烯酸酯(TEGDMA)的量均无影响。与对照样品相比,从漂白后的Ceram X样品中释放的双酚A的量显著降低。漂白显著减少了从Filtek Supreme XT中释放的Bis-GMA的量。从Filtek Supreme XT中释放的TEGDMA的量不受漂白影响。
本研究中测试的漂白剂减少了从两种复合材料中释放的一些单体的量。现代复合材料的漂白不会增加单体的释放。