Smith F E, Arsenault E A
Talanta. 1996 Aug;43(8):1207-68. doi: 10.1016/0039-9140(96)01882-6.
The speed and efficiency of instrumentation for chemical analysis has improved dramatically over the past twenty years. Until recently, however, methods of sample preparation had not changed to keep pace, so this had become the slowest step in analytical chemistry methodology. The widespread adoption of domestic microwave ovens during the past twenty-five years has eventually led to their usage in chemical laboratories. Microwave technology has now advanced to the point where it is revolutionizing chemical sample preparation and chemical synthesis. Since the first application of a microwave oven for sample preparation in 1975, many microwave-assisted dissolution methods have been developed - these are applicable to virtually any kind of sample type. This review attempts to summarize all the microwave-assisted dissolution and digestion methods reported up to and including 1994. In addition, some very recent developments in continuous-flow automated dissolution systems are discussed, as is the emergence of databases and software packages related to the application of microwave technology to sample dissolution. There are 344 references.
在过去二十年中，化学分析仪器的速度和效率有了显著提高。然而，直到最近，样品制备方法却没有跟上步伐，因此这已成为分析化学方法中最慢的步骤。在过去二十五年里，家用微波炉的广泛使用最终使其进入了化学实验室。如今，微波技术已发展到正在彻底改变化学样品制备和化学合成的程度。自1975年微波炉首次应用于样品制备以来，已开发出许多微波辅助溶解方法——这些方法几乎适用于任何类型的样品。本综述试图总结截至1994年（包括1994年）所报道的所有微波辅助溶解和消解方法。此外，还讨论了连续流动自动溶解系统的一些最新进展，以及与微波技术在样品溶解中的应用相关的数据库和软件包的出现。本文有344篇参考文献。
