一种用于合成亚胺氮化硅整体凝胶和高比表面积气凝胶的非氧化物溶胶-凝胶法。
A non-oxide sol-gel route to synthesise silicon imidonitride monolithic gels and high surface area aerogels.
作者信息
Hassan Shereen, Hector Andrew L, Hyde Jason R, Kalaji Ali, Smith David C
机构信息
School of Chemistry, University of Southampton, Highfield, Southampton, UK.
出版信息
Chem Commun (Camb). 2008 Nov 14(42):5304-6. doi: 10.1039/b810317h. Epub 2008 Sep 12.
DOI:10.1039/b810317h
PMID:18985191
Abstract
Monolithic gels have been produced by reaction of Si(NHMe)(4) with ammonia in THF solution and converted to high surface area aerogels by critical point drying with ammonia saturated diethylamine solvent.
摘要
通过在四氢呋喃溶液中使硅（N-甲基亚氨基）（4）与氨反应制备了整体凝胶，并通过用氨饱和的二乙胺溶剂进行临界点干燥将其转化为高表面积气凝胶。
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