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基于第二代同步辐射源的高分辨率硬X射线显微镜。

High resolution hard x-ray microscope on a second generation synchrotron source.

作者信息

Tian Yangchao, Li Wenjie, Chen Jie, Liu Longhua, Liu Gang, Tkachuk Andrei, Tian Jinping, Xiong Ying, Gelb Jeff, Hsu George, Yun Wenbing

机构信息

National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei Anhui 230029, People's Republic of China.

出版信息

Rev Sci Instrum. 2008 Oct;79(10):103708. doi: 10.1063/1.3002484.

Abstract

A full-field, transmission x-ray microscope (TXM) operating in the energy range of 7-11 keV has been installed at the U7A beamline at the National Synchrotron Radiation Laboratory, a second generation synchrotron source operating at 0.8 GeV. Although the photon flux at sample position in the operating energy range is significantly low due to its relatively large emittance, the TXM can get high quality x-ray images with a spatial resolution down to 50 nm with acceptable exposure time. This TXM operates in either absorption or Zernike phase contrast mode with similar resolution. This TXM is a powerful analytical tool for a wide range of scientific areas, especially studies on nanoscale phenomena and structural imaging in biology, materials science, and environmental science. We present here the property of the x-ray source, beamline design, and the operation and key optical components of the x-ray TXM. Plans to improve the throughput of the TXM will be discussed.

摘要

一台工作在7 - 11千电子伏特能量范围内的全场透射式X射线显微镜(TXM)已安装在国家同步辐射实验室的U7A光束线上,该实验室是一台运行能量为0.8 GeV的第二代同步辐射源。尽管由于其相对较大的发射度,在工作能量范围内样品位置处的光子通量显著较低,但TXM在可接受的曝光时间下能够获得空间分辨率低至50纳米的高质量X射线图像。这台TXM以吸收或泽尼克相衬模式运行,分辨率相似。这台TXM是用于广泛科学领域的强大分析工具,特别是在生物学、材料科学和环境科学中对纳米尺度现象和结构成像的研究。我们在此介绍X射线源的特性、光束线设计以及X射线TXM的操作和关键光学组件。还将讨论提高TXM通量的计划。

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