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用作舌侧保持器粘合剂的含无定形磷酸钙正畸复合材料的粘结强度

Bond strength of amorphous calcium phosphate-containing orthodontic composite used as a lingual retainer adhesive.

作者信息

Uysal Tancan, Ulker Mustafa, Akdogan Gulsen, Ramoglu Sabri Ilhan, Yilmaz Esra

机构信息

Department of Orthodontics, Erciyes University, Kayseri, Turkey.

出版信息

Angle Orthod. 2009 Jan;79(1):117-21. doi: 10.2319/112807-560.1.

Abstract

OBJECTIVE

To evaluate the shear bond strength and fracture mode difference between amorphous calcium phosphate (ACP)-containing adhesive and conventional resin-based composite material used as an orthodontic lingual retainer adhesive.

MATERIALS AND METHODS

Forty crowns of extracted lower human incisors were mounted in acrylic resin, leaving the buccal surface of the crowns parallel to the base of the molds. The teeth were randomly divided into two groups: experimental and control, containing 20 teeth each. Conventional lingual retainer composite (Transbond-LR, 3M-Unitek) and ACP-containing orthodontic adhesive (Aegis-Ortho) were applied to the teeth surface by packing the material into the cylindrical plastic matrices with a 2.34-mm internal diameter and a 3-mm height (Ultradent) to simulate the lingual retainer bonding. For shear bond testing, the specimens were mounted in a universal testing machine, and an apparatus (Ultradent) attached to a compression load cell was applied to each specimen until failure occurred. The shear bond data were analyzed using Student's t-test. Fracture modes were analyzed by chi(2) test.

RESULTS

The statistical test showed that the bond strengths of group 1 (control Transbond-LR, mean: 24.77 +/- 9.25 MPa) and group 2 (ACP-containing adhesive, mean: 8.49 +/- 2.53 MPa) were significantly different from each other. In general, a greater percentage of the fractures were adhesive at the tooth-composite interface (60% in group 1 and 55% in group 2), and no statistically significant difference was found between groups.

CONCLUSION

The ACP-containing Aegis-Ortho adhesive resulted in a significant decrease in bond strength to the etched enamel surface.

摘要

目的

评估含无定形磷酸钙(ACP)的黏合剂与用作正畸舌侧保持器黏合剂的传统树脂基复合材料之间的剪切黏结强度及断裂模式差异。

材料与方法

将40颗拔除的人下颌切牙冠固定于丙烯酸树脂中,使牙冠的颊面与模具底部平行。牙齿随机分为两组:实验组和对照组,每组20颗牙。将传统舌侧保持器复合材料(Transbond-LR,3M-Unitek)和含ACP的正畸黏合剂(Aegis-Ortho)通过将材料填充到内径2.34 mm、高3 mm的圆柱形塑料基质(Ultradent)中,涂抹于牙齿表面,以模拟舌侧保持器黏结。对于剪切黏结测试,将标本安装在万能试验机上,使用连接到压缩测力传感器的装置(Ultradent)对每个标本施加力直至发生破坏。使用学生t检验分析剪切黏结数据。通过卡方检验分析断裂模式。

结果

统计检验表明,第1组(对照Transbond-LR,均值:24.77±9.25 MPa)和第2组(含ACP的黏合剂,均值:8.49±2.53 MPa)的黏结强度存在显著差异。总体而言,在牙齿-复合材料界面,更大比例的断裂为黏附性断裂(第1组为60%,第2组为55%),两组之间未发现统计学上的显著差异。

结论

含ACP的Aegis-Ortho黏合剂导致与酸蚀釉质表面的黏结强度显著降低。

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