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[对锡金白粉藤化学成分的研究]

[Studies on the chemical constituents from Cissus assamica].

作者信息

Xie Yi-hui, Deng Peng, Zhang Ye-qing, Yu Wu-shuang

机构信息

Jiangxi College of TCM, Nanchang 330006, China.

出版信息

Zhong Yao Cai. 2009 Feb;32(2):210-3.

Abstract

OBJECTIVE

To study the chemical constituents from Cissus assamica and obtain a more comprehensive understanding of its effective components.

METHODS

Compounds were isolated by various column chromatographies with silica gel. Their structures were elucidated by spectral analysis (IR, MS, 1H-NMR, 13C-NMR) and chemical evidence.

RESULTS

Eight compounds were isolated and elucidated as ursolic acid (I), lupeol (II), n-hexacosinc acid (III), isolariciresinol-9-O-beta-D-glucopyranoside (IV), dauco sterin (V), 3,3'-dimethyl ellagic acid (VI), beta-Sitosterol (VII), bergenin (VIII).

CONCLUSION

Among these compounds, I-V are isolated from this plant for the first time.

摘要

目的

研究锡金白粉藤的化学成分,更全面地了解其有效成分。

方法

采用多种硅胶柱色谱法分离化合物。通过光谱分析(红外光谱、质谱、¹H-核磁共振、¹³C-核磁共振)和化学证据阐明其结构。

结果

分离鉴定出8个化合物,分别为熊果酸(Ⅰ)、羽扇豆醇(Ⅱ)、正二十六碳酸(Ⅲ)、异落叶松脂素-9-O-β-D-吡喃葡萄糖苷(Ⅳ)、胡萝卜苷(Ⅴ)、3,3'-二甲基鞣花酸(Ⅵ)、β-谷甾醇(Ⅶ)、岩白菜素(Ⅷ)。

结论

这些化合物中,Ⅰ-Ⅴ为首次从该植物中分离得到。

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