Chuang Shu-Fen, Chen Hui-Ping, Chang Chih-Han, Liu Jia-Kuang
Institute of Oral Medicine, National Cheng Kung University, Tainan, Taiwan.
Eur J Oral Sci. 2009 Aug;117(4):435-41. doi: 10.1111/j.1600-0722.2009.00645.x.
The aim of this study was to examine the resin bond strength on enamel treated with different fluoridated bleaching agents. Forty-eight bovine incisors were divided into four groups to receive bleaching treatments, over a 14-d period, as follows: no treatment; 10% carbamide peroxide (CP) bleaching; 10% CP containing 0.11% fluoride; and 10% CP containing 0.37% fluoride. Immediately, and 7 and 14 d after bleaching, the enamel surfaces were respectively bonded with composite and sectioned to create resin-enamel beams. These beams were subjected to the microtensile bond strength (microTBS) test, then assessed for failure mode under scanning electron microscopy. The results showed that the 0.37% fluoridated group demonstrated a microTBS equivalent to that of the unbleached group at all stages. Non-fluoridated and 0.11% fluoridated groups showed a weaker microTBS after bleaching but regained the bond strength after 14 or 7 d of storage, respectively. In the non-fluoridated group, adhesive failure was the predominant fracture pattern that comprised the enamel prism demineralization change and widely dispersed voids on the resin-enamel interfaces. No evident enamel erosion and fewer microporosities were found in the 0.37% fluoridated group. Accordingly, treatment with 0.37% fluoridated CP maintained the microTBS as effectively as the unbleached enamel. Additional fluoride in the bleaching agents may facilitate subsequent restorative treatment by inhibiting enamel demineralization.
本研究的目的是检测用不同含氟漂白剂处理过的牙釉质上的树脂粘结强度。48颗牛切牙被分为四组,在14天的时间里接受如下漂白处理:不处理;10%过氧化脲(CP)漂白;含0.11%氟的10% CP;以及含0.37%氟的10% CP。在漂白后即刻、7天和14天,牙釉质表面分别与复合材料粘结,然后切片制成树脂-牙釉质梁。对这些梁进行微拉伸粘结强度(microTBS)测试,然后在扫描电子显微镜下评估破坏模式。结果表明,0.37%含氟组在所有阶段的微拉伸粘结强度均与未漂白组相当。未含氟组和含0.11%氟组在漂白后微拉伸粘结强度较弱,但分别在储存14天或7天后恢复了粘结强度。在未含氟组中,粘结失败是主要的断裂模式,包括牙釉质棱柱脱矿变化以及树脂-牙釉质界面上广泛分布的空隙。在0.37%含氟组中未发现明显的牙釉质侵蚀且微孔较少。因此,用0.37%含氟CP处理能像未漂白牙釉质一样有效地维持微拉伸粘结强度。漂白剂中额外的氟可能通过抑制牙釉质脱矿促进后续的修复治疗。