Torrezan A C, Mayer Alegre T P, Medeiros-Ribeiro G
Laboratório Nacional de Luz Síncrotron, Caixa Postal 6192, Campinas, São Paulo 13084-971, Brazil.
Rev Sci Instrum. 2009 Jul;80(7):075111. doi: 10.1063/1.3186054.
In this article we evaluate the performance of an electron paramagnetic resonance (EPR) setup using a microstrip resonator (MR). The design and characterization of the resonator are described and parameters of importance to EPR and spin manipulation are examined, including cavity quality factor, filling factor, and microwave magnetic field in the sample region. Simulated microwave electric and magnetic field distributions in the resonator are also presented and compared with qualitative measurements of the field distribution obtained by a perturbation technique. Based on EPR experiments carried out with a standard marker at room temperature and a MR resonating at 8.17 GHz, the minimum detectable number of spins was found to be 5 x 10(10) spins/GHz(1/2) despite the low MR unloaded quality factor Q0=60. The functionality of the EPR setup was further evaluated at low temperature, where the spin resonance of Cr dopants present in a GaAs wafer was detected at 2.3 K. The design and characterization of a more versatile MR targeting an improved EPR sensitivity and featuring an integrated biasing circuit for the study of samples that require an electrical contact are also discussed.
在本文中,我们评估了一种使用微带谐振器(MR)的电子顺磁共振(EPR)装置的性能。描述了谐振器的设计与特性,并研究了对EPR和自旋操控至关重要的参数,包括腔品质因数、填充因数以及样品区域内的微波磁场。还给出了谐振器中模拟的微波电场和磁场分布,并与通过微扰技术获得的场分布定性测量结果进行了比较。基于在室温下用标准标记物以及在8.17 GHz谐振的MR进行的EPR实验,尽管MR的空载品质因数Q0 = 60较低,但发现最小可检测自旋数为5×10(10) 自旋/GHz(1/2)。在低温下进一步评估了EPR装置的功能,在2.3 K时检测到了砷化镓晶片中存在的Cr掺杂剂的自旋共振。还讨论了一种更通用的MR的设计与特性,该MR旨在提高EPR灵敏度,并具有用于研究需要电接触的样品的集成偏置电路。