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自粘接树脂水门汀体外磨损间隙形成:CLSM 评价。

In vitro wear gap formation of self-adhesive resin cements: a CLSM evaluation.

机构信息

Department of Operative Dentistry, School of Dentistry, Federal University of Santa Catarina, Brazil.

出版信息

J Dent. 2009 Dec;37(12):984-93. doi: 10.1016/j.jdent.2009.08.006. Epub 2009 Aug 20.

Abstract

OBJECTIVES

To evaluate the depth of wear gaps of new self-adhesive cements after toothbrush abrasion and ACTA wear test.

METHODS

Luting spaces (325+/-25 microm width, 2mm depth) were produced in Empress 2 ceramic blocks with a diamond saw to obtain flat substrate segments for toothbrush abrasion (n=24) and ACTA wear (n=27). After etching and silanization, the slits were filled with 8 self-adhesive cements, 2 conventional resin cements and 1 flowable composite, stored for 2 weeks in distilled water at 37 degrees C and planished to the cement level. Toothbrush abrasion was carried out in a toothbrush simulator (Willytec, Germany) for 20,000 cycles (load 1N) using an abrasive slurry based on a commercial toothpaste (Elmex, Gaba, Germany, RDA=77). The ACTA wear experiment was performed following the ACTA protocol in millet seed slurry for 400,000 cycles (Willytec). The gap replicas were measured for vertical wear loss under a confocal laser scanning microscope (CLSM). The data were analyzed using one-way ANOVA and a mod-LSD test at p<0.05.

RESULTS

Toothbrush wear values were lower than the ones obtained for the ACTA wear test for all cements. In the toothbrush test Bifix SE, Clearfil SA, SmartCem 2, G-Cem and Maxcem Elite obtained the highest values together with Grandio Flow. Grandio Flow and AllCem showed to be the most resistant to the ACTA wear test, while SpeedCem the least resistant. No correlation was found between the two wear test experiments.

CONCLUSION

Self-adhesive cements have good wear resistance to toothbrush abrasion but most of them wear more rapidly under higher loads in the ACTA test than conventional resin cements and flowable composites.

摘要

目的

评估新自粘接水门汀在牙刷磨损和 ACTA 磨损试验后的磨损间隙深度。

方法

用金刚石锯在 Empress 2 陶瓷块上制备宽 325+/-25 微米、深 2 毫米的粘固间隙,以获得用于牙刷磨损(n=24)和 ACTA 磨损(n=27)的平面基底段。蚀刻和硅烷化后,用 8 种自粘接水门汀、2 种传统树脂水门汀和 1 种流动复合树脂填充狭缝,在 37°C 蒸馏水中储存 2 周,然后用平面仪将其压平至与水门汀平齐。在 Willytec(德国)牙刷模拟器上进行牙刷磨损试验,用商业牙膏(德国 Gaba 的 Elmex,RDA=77)制成的磨料浆进行 20000 次循环(负载 1N)。按照 ACTA 方案,在 millet 种子浆中进行 400000 次循环(Willytec)的 ACTA 磨损试验。用共聚焦激光扫描显微镜(CLSM)测量间隙复制体的垂直磨损损失。使用单向方差分析和 mod-LSD 检验,p<0.05 时进行数据分析。

结果

所有水门汀的牙刷磨损值均低于 ACTA 磨损试验的磨损值。在牙刷试验中,Bifix SE、Clearfil SA、SmartCem 2、G-Cem 和 Maxcem Elite 与 Grandio Flow 一起获得了最高值。Grandio Flow 和 AllCem 显示出对 ACTA 磨损试验的抵抗力最强,而 SpeedCem 则抵抗力最弱。两种磨损试验之间未发现相关性。

结论

自粘接水门汀对牙刷磨损具有良好的耐磨性,但在 ACTA 试验中,它们在较高负荷下的磨损速度比传统树脂水门汀和流动复合树脂更快。

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