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采用带氮特异性检测的气相色谱法和质谱法对兴奋剂和麻醉性镇痛药进行系统分析。

Systematic analysis of stimulants and narcotic analgesics by gas chromatography with nitrogen specific detection and mass spectrometry.

作者信息

Lho D S, Shin H S, Kang B K, Park J

机构信息

Doping Control Center, Korea Institute of Science and Technology, Cheongryang, Seoul.

出版信息

J Anal Toxicol. 1990 Mar-Apr;14(2):73-6. doi: 10.1093/jat/14.2.73.

DOI:10.1093/jat/14.2.73
PMID:1969975
Abstract

The recovery data of 40 doping agents from human urine were evaluated. Retention data were standardized by the calculation of relative retention times using N,N-diisopropyl-n-dodecane as the internal standard. The relative standard deviations of retention times were less than 0.5% for the within batch analyses and less than 0.8% for the day-to-day analyses. Good recoveries (greater than 70%) were observed for most of the drugs.

摘要

对40种兴奋剂在人尿中的回收率数据进行了评估。保留数据通过使用N,N-二异丙基正十二烷作为内标计算相对保留时间进行标准化。批内分析中保留时间的相对标准偏差小于0.5%,日常分析中小于0.8%。大多数药物的回收率良好(大于70%)。

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