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甲基丙烯酸树脂抛光标准化方法的性能分析

Analysis of the performance of a standardized method for the polishing of methacrylic resins.

作者信息

Corsalini Massimo, Boccaccio Antonio, Lamberti Luciano, Pappalettere Carmine, Catapano Santo, Carossa Stefano

机构信息

School of Dentistry, University of Bari, Bari, Italy.

出版信息

Open Dent J. 2009 Dec 4;3:233-40. doi: 10.2174/1874210600903010233.

Abstract

Adhesion of micro-organisms to resin surface may be caused by inadequate polishing. Most of the studies published in literature are relative to manually prepared samples and do not take into account that test repeatability is not guaranteed a priori since skills may change from one operator to another and the quality of the work done by the same expert operator may depend on "human" factors such as the level of attention, wrist trembling, etc.This paper aims to investigate on the efficiency and reliability of a standardized protocol for polishing methacrylic resins. For that purpose, five different methacrylic resins are considered. For each resin, 20 specimens are realized: 10 are polished by the same expert operator and 10 are polished by means of a mechanical system comprised of a milling tool, a mobile support for samples and a micrometric advance isoparallelometer. Roughness measurements are carried out with a +/-0.01 microm resolution profilometer. An extensive statistical analysis is conducted on a population of 100 specimens. Two-way Analysis of Variance (ANOVA) is carried out taking the type of resin (i) and the polishing technique (ii) as predictors in order to evaluate how those variables will finally affect the roughness of the polished surface. The significance of the variable interaction term is assessed. The null hypothesis Ho where response is independent from individual factors as well as from their interaction is assumed to hold true for p-values>0.05 (interval of confidence of the 95%). Experimental data confirm that mechanical polishing leads to obtaining surfaces of much more uniform quality. In fact, statistical dispersion of roughness parameters can decrease significantly. This behavior is observed for all of the tested resins. Therefore, the new approach can eliminate the influence of "human" factors thus making it possible to assess the inherent features of each resin and compare different dental materials submitted to polishing.

摘要

微生物附着于树脂表面可能是由抛光不足所致。文献中发表的大多数研究都与人工制备的样本相关,且未考虑到由于不同操作人员的技能可能不同,以及同一专业操作人员的工作质量可能取决于诸如注意力水平、手腕颤抖等“人为”因素,因此无法事先保证测试的可重复性。本文旨在研究一种用于抛光甲基丙烯酸树脂的标准化方案的效率和可靠性。为此,考虑了五种不同的甲基丙烯酸树脂。对于每种树脂,制作20个样本:10个由同一位专业操作人员抛光,10个通过由铣刀、样本移动支架和测微平行进刀仪组成的机械系统进行抛光。使用分辨率为±0.01微米的轮廓仪进行粗糙度测量。对100个样本进行了广泛的统计分析。以树脂类型(i)和抛光技术(ii)作为预测变量进行双向方差分析(ANOVA),以评估这些变量最终将如何影响抛光表面的粗糙度。评估变量交互项的显著性。对于p值>0.05(95%的置信区间),假定响应与个体因素及其交互作用无关的原假设Ho成立。实验数据证实,机械抛光可使表面质量更加均匀。事实上,粗糙度参数的统计离散度可显著降低。在所有测试树脂中均观察到这种现象。因此,新方法可以消除“人为”因素的影响,从而能够评估每种树脂的固有特性,并比较经过抛光的不同牙科材料。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3b98/2808027/e0f1bd51764a/TODENTJ-3-233_F1.jpg

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