Hou T W, Mogab C J
Appl Opt. 1981 Sep 15;20(18):3184-8. doi: 10.1364/AO.20.003184.
The prism coupling technique has been used to measure the refractive index and thickness of plasma silicon oxide films deposited on garnet substrates. The film thickness is also measured with a mechanical stylus (Talystep) for comparison. A linearly polarized He-Ne laser at 632.8-nm wavelength or a He-Cd laser at 441.6-nm wavelength is used as the light source in the prism coupler. The use of the He-Ne laser is demonstrated to result in a fluctuation in the detector output due to light interference in the substrate. The He-Cd laser is shown to be superior because the substrate is sufficiently absorbing that interference is eliminated. It also permits thickness measurements on thinner films. The agreement between thickness measurements by the prism coupler and the mechanical stylus is within +/-0.015 microm for films of 0.4 microm or thicker and +/-0.010 microm for thinner films. The error in thickness measurement caused by an error in refractive index assumed or in determining the coupling angles for films thinner than 0.30 microm is also estimated.
棱镜耦合技术已被用于测量沉积在石榴石衬底上的等离子体氧化硅薄膜的折射率和厚度。薄膜厚度也用机械探针(Talystep)进行测量以便比较。在棱镜耦合器中,使用波长为632.8纳米的线偏振氦氖激光器或波长为441.6纳米的氦镉激光器作为光源。结果表明,使用氦氖激光器会由于衬底中的光干涉而导致探测器输出出现波动。氦镉激光器表现更优,因为衬底有足够的吸收能力从而消除了干涉。它还允许对更薄的薄膜进行厚度测量。对于厚度为0.4微米或更厚的薄膜,棱镜耦合器和机械探针测量的厚度之间的偏差在±0.015微米以内,对于更薄的薄膜,偏差在±0.010微米以内。还估算了对于厚度小于0.30微米的薄膜,由于假设的折射率误差或确定耦合角时的误差所导致的厚度测量误差。