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A simple external resistance heating diamond anvil cell and its application for synchrotron radiation x-ray diffraction.

作者信息

Fan Dawei, Zhou Wenge, Wei Shuyi, Liu Yonggang, Ma Maining, Xie Hongsen

机构信息

Institute of Geochemistry of Earth's Deep Interior Materials and Fluid Interaction, Chinese Academy of Sciences, Guiyang 550002, China.

出版信息

Rev Sci Instrum. 2010 May;81(5):053903. doi: 10.1063/1.3430069.

Abstract

A simple external heating assemblage allowing diamond anvil cell experiments at pressures up to 34 GPa and temperatures up to 653 K was constructed. This cell can be connected to the synchrotron radiation conveniently. The design and construction of this cell are fully described, as well as its applications for x-ray diffraction. Heating is carried out by using an external-heating system, which is made of NiCr resistance wire, and the temperature was measured by a NiCr-NiSi or PtRh-Pt thermocouple. We showed the performance of the new system by introducing the phase transition study of cinnabar (alpha-HgS) and thermal equation of state study of almandine at high pressure and temperature with this cell.

摘要

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