Guida M, Palmisano C
Università di Torino, Dipartimento di Fisica Generale A. Avogadro, via P. Giuria 1, 10125 Torino, Italy.
Acta Crystallogr A. 2010 Jul;66(Pt 4):470-8. doi: 10.1107/S0108767310011256. Epub 2010 May 7.
This paper is a study of surface effects, e.g. roughness or asymmetrical cut, in the Laue diffraction of X-rays by crystals, based on the Takagi-Taupin equations. By means of Riemann-Green integrals, first a formal solution has been obtained when the entrance and the exit surfaces are arbitrary. Then a coordinate transformation mapping a propagation domain with arbitrary boundaries into a rectangular domain with straight boundaries is given. Potential measurement errors in \gamma-ray wavelength and silicon lattice-parameter measurements by double-crystal diffractometry and X-ray interferometry, respectively, are outlined and anticipated by studying, in the two-wave approximation, the reflection peak shift and extra phase originating from an asymmetrically cut crystal. A relationship between analyser displacement, interferometer-signal phase and relative uncertainty in lattice-parameter measurement is also given.
本文基于高木-田品方程,研究了晶体对X射线劳厄衍射中的表面效应,例如粗糙度或不对称切割。通过黎曼-格林积分,首先在入射面和出射面为任意面时得到了形式解。然后给出了一种坐标变换,将具有任意边界的传播域映射为具有直边界的矩形域。通过在双波近似下研究由不对称切割晶体引起的反射峰位移和额外相位,分别概述并预测了在γ射线波长测量和硅晶格参数测量中,使用双晶衍射仪和X射线干涉仪时潜在的测量误差。还给出了分析器位移、干涉仪信号相位与晶格参数测量相对不确定度之间的关系。