Anhui Province Key Laboratory of Research and Development of Chinese Medicine, School of Life Sciences, Anhui University, Hefei 230039, PR China.
Fitoterapia. 2010 Oct;81(7):869-72. doi: 10.1016/j.fitote.2010.05.012. Epub 2010 May 23.
Two new norlignan derivatives, crassifoside I (1) and sinensigenin C (2), were isolated from the rhizomes of Curculigo capitulate, along with six known norlignan derivatives, 1,1-bis(3,4-dihydroxyphenyl)-1-(2-furan)-methane (3), crassifogenin B (4), crassifoside A (5), breviscaside A (6), crassifoside D (7), and curcapital (8). Their structures were elucidated on the basis of spectral evidence and comparisons with literature data. The 1H and 13C NMR data of compound 3 was first assigned. Compounds 3-7 were isolated from this plant for the first time.
两种新的木脂素衍生物,crassifoside I(1)和sinensigenin C(2),从 Curculigo capitulate 的根茎中分离出来,此外还有六种已知的木脂素衍生物,1,1-双(3,4-二羟基苯基)-1-(2-呋喃)-甲烷(3),cras sifogenin B(4),cras sifoside A(5),breviscaside A(6),cras sifoside D(7)和 curcapital(8)。基于光谱证据和与文献数据的比较,确定了它们的结构。首次分配了化合物 3 的 1H 和 13C NMR 数据。化合物 3-7 也是首次从该植物中分离得到。