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微量热计的测试与校准过程,特别涉及与水体系一起使用的热传导仪器。

Test and calibration processes for microcalorimeters, with special reference to heat conduction instruments used with aqueous systems.

作者信息

Briggner L E, Wadsö I

机构信息

Division of Thermochemistry, University of Lund, Sweden.

出版信息

J Biochem Biophys Methods. 1991 Feb-Mar;22(2):101-18. doi: 10.1016/0165-022x(91)90023-p.

DOI:10.1016/0165-022x(91)90023-p
PMID:2061558
Abstract

Calorimeters are normally calibrated by use of electrical heaters, but the calibration values derived may not always be representative for the chemical or biological process investigated. It is therefore important to have available chemical test processes by which the electrical calibration values can be controlled. In some cases, electrical calibration should be replaced by chemical calibrations. With particular reference to needs in work with thermophile heat conduction microcalorimeters, a number of test and calibration processes are presented. Some calibration problems for various types of reaction vessel are discussed.

摘要

热量计通常通过使用电加热器进行校准,但由此得出的校准值可能并不总是能代表所研究的化学或生物过程。因此,拥有可用于控制电校准值的化学测试过程非常重要。在某些情况下,应将电校准替换为化学校准。特别针对嗜热导热微量热计的工作需求,介绍了一些测试和校准过程。讨论了各种类型反应容器的一些校准问题。

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