[Preparation of monodesethylamodiaquine from human urine].
作者信息
Ménager S, Lafont O, Chrétien P, Bryskier A
机构信息
Groupe de Pharmacochimie, Faculté de Médecine, Saint-Etienne-du-Rouvray.
出版信息
Ann Pharm Fr. 1990;48(1):38-41.
PMID:2082800
Abstract
60 mg of monodesethylamodiaquine, the active metabolite of amodiaquine were prepared by extraction from human urine, at pH 11-12, using ethyl acetate. The purification was carried out by medium pressure liquid chromatography. The identity and the purity of the compound were checked by thin layer chromatography, 1H nuclear magnetic resonance and mass spectrometry.
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