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采用顶空固相微萃取法测定啤酒香气成分。

Determination of beer aroma compounds using headspace solid-phase microcolumn extraction.

机构信息

The Plant Production Research Center Piešťany, Institute of Viticulture and Enology, Matúškova 25, 831 01 Bratislava, Slovak Republic.

出版信息

Talanta. 2010 Nov 15;83(1):294-6. doi: 10.1016/j.talanta.2010.08.041. Epub 2010 Sep 9.

DOI:10.1016/j.talanta.2010.08.041
PMID:21035679
Abstract

A rapid sampling technique for the analysis of beer aroma compounds is described. The headspace (10 ml) is passed through the microcolumn filled with 5mg of Tenax TA and thermally desorbed in a modified GC inlet (modification is described). Eight compounds (from acetaldehyde to 2-phenylethanol) in four beer samples were analyzed. The correlation coefficients (r(2)), repeatability (RSD) and limits of detection (LOD) were 0.9973-0.9994, 2.1-6.9% and 0.00002-0.13 mg/l, respectively. The methodology can be useful for routine beer sample analysis.

摘要

一种快速采样技术用于分析啤酒香气化合物。顶空(10 毫升)通过填充有 5mg Tenax TA 的微柱,在改进的 GC 进样口(描述了改进)中热解吸。四个啤酒样品中分析了八种化合物(从乙醛到 2-苯乙醇)。相关系数(r(2))、重复性(RSD)和检测限(LOD)分别为 0.9973-0.9994、2.1-6.9%和 0.00002-0.13mg/L。该方法可用于常规啤酒样品分析。

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