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体外牙科硅氧烷的可修复性。

Repairability of dental siloranes in vitro.

机构信息

Department of Conservative Dentistry, Periodontology and Preventive Dentistry, Hannover Medical School, Hannover, Germany.

出版信息

Dent Mater. 2011 Feb;27(2):144-9. doi: 10.1016/j.dental.2010.09.009. Epub 2010 Nov 2.

Abstract

OBJECTIVES

Aim of the study was the investigation of the repairability of a silorane (Filtek Silorane, 3M Espe, Seefeld, Germany) after different surface pretreatments in vitro.

METHODS

54 silorane specimens (5 mm × 5 mm × 5 mm) were fabricated and stored in saline solution (24 h/37°C). Their surface was polished with abrasive paper (600 grit), etched with phosphoric acid (10 s) and rinsed with water (30 s). Repair was performed with a silorane based on one of the 9 treatment protocols (each n=6): no additional treatment (NAT), silorane primer (P) and silorane bond (B), B only, sandblasting (SB), SB plus P/B, SB plus B, CoJet and silane (CJ), CJ plus P/B, CJ plus B. Whole silorane specimens (5 mm × 5 mm × 10 mm) with no repair served as control. Specimens were sectioned and microtensile bond strength (μTBS) was measured (30 beams per group, surface area approx. 1.2 mm², crosshead-speed 1 mm/min) statistical analysis (ANOVA, Tukey HSD, p<0.05) was performed.

RESULTS

μTBS of the specimens was significantly influenced by the surface pretreatment (p<0.001). The highest μTBS was determined for CJ/B and SB/B, which were not significantly different from the control. NAT, SB and CJ benefited from an additional treatment with B (p<0.01). The additional use of P did not improve μTBS, but was detrimental for the SB and CJ groups (p<0.05).

SIGNIFICANCE

Siloranes can be repaired with either SB or CJ in combination with a silorane bond, the additional use of silorane primer is disadvantageous.

摘要

目的

本研究的目的是体外研究不同表面预处理对硅烷(Filtek Silorane,3M Espe,Seefeld,德国)的可修复性。

方法

制备 54 个硅烷试件(5mm×5mm×5mm)并储存在盐溶液中(24h/37°C)。用研磨砂纸(600 目)对试件表面进行抛光,用磷酸蚀刻(10s)并用去离子水冲洗(30s)。采用基于以下 9 种处理方案之一的硅烷进行修复(每组 n=6):无附加处理(NAT)、硅烷底漆(P)和硅烷粘结剂(B)、仅 B、喷砂(SB)、SB 加 P/B、SB 加 B、CoJet 加硅烷(CJ)和硅烷(CJ)加 P/B、CJ 加 B。未修复的全硅烷试件(5mm×5mm×10mm)作为对照。对试件进行切片,测量微拉伸粘结强度(μTBS)(每组 30 个梁,表面积约 1.2mm²,十字头速度 1mm/min),进行统计分析(ANOVA,Tukey HSD,p<0.05)。

结果

试件的 μTBS 显著受表面预处理影响(p<0.001)。CJ/B 和 SB/B 的 μTBS 最高,与对照组无显著差异。NAT、SB 和 CJ 经 B 处理后受益(p<0.01)。P 的额外使用并未提高 μTBS,但对 SB 和 CJ 组不利(p<0.05)。

意义

硅烷可通过 SB 或 CJ 与硅烷粘结剂联合修复,硅烷底漆的额外使用不利。

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