Piracicaba Dental School, Department of Restorative Dentistry, University of Campinas-UNICAMP, Piracicaba, SP, Brazil.
Lasers Med Sci. 2012 Jan;27(1):145-51. doi: 10.1007/s10103-010-0857-y. Epub 2010 Nov 23.
The aim of this study was to evaluate the influence of different curing lights and chemical catalysts on the degree of conversion of resin luting cements. A total of 60 disk-shaped specimens of RelyX ARC or Panavia F of diameter 5 mm and thickness 0.5 mm were prepared and the respective chemical catalyst (Scotchbond Multi-Purpose Plus or ED Primer) was added. The specimens were light-cured using different curing units (an argon ion laser, an LED or a quartz-tungsten-halogen light) through shade A2 composite disks of diameter 10 mm and thickness 2 mm. After 24 h of dry storage at 37°C, the degree of conversion of the resin luting cements was measured by Fourier-transformed infrared spectroscopy. For statistical analysis, ANOVA and the Tukey test were used, with p ≤ 0.05. Panavia F when used without catalyst and cured using the LED or the argon ion laser showed degree of conversion values significantly lower than RelyX ARC, with and without catalyst, and cured with any of the light sources. Therefore, the degree of conversion of Panavia F with ED Primer cured with the quartz-tungsten-halogen light was significantly different from that of RelyX ARC regardless of the use of the chemical catalyst and light curing source. In conclusion, RelyX ARC can be cured satisfactorily with the argon ion laser, LED or quartz-tungsten-halogen light with or without a chemical catalyst. To obtain a satisfactory degree of conversion, Panavia F luting cement should be used with ED Primer and cured with halogen light.
本研究旨在评估不同固化灯和化学催化剂对树脂水门汀聚合程度的影响。共制备了 60 个直径为 5mm、厚度为 0.5mm 的 RelyX ARC 或 Panavia F 圆盘试件,并分别加入相应的化学催化剂(Scotchbond Multi-Purpose Plus 或 ED Primer)。使用不同的固化装置(氩离子激光、LED 或石英钨卤灯),通过直径为 10mm、厚度为 2mm 的 A2 遮色复合树脂片对试件进行光固化。37°C 干燥储存 24h 后,采用傅里叶变换红外光谱法测量树脂水门汀的聚合程度。采用方差分析和 Tukey 检验进行统计学分析,p≤0.05。未加催化剂且使用 LED 或氩离子激光固化的 Panavia F 的聚合程度值明显低于加催化剂和不加催化剂、使用任何光源固化的 RelyX ARC。因此,无论是否使用化学催化剂以及光源,ED Primer 固化的 Panavia F 与 RelyX ARC 的聚合程度均有显著差异。结论:RelyX ARC 可分别使用氩离子激光、LED 或石英钨卤灯,并可加或不加化学催化剂进行充分固化。为了获得令人满意的聚合程度,Panavia F 水门汀应与 ED Primer 联合使用,并采用卤素灯进行固化。