Advanced Materials and Nanotechnology Laboratory, Institute of Advanced Technology (ITMA), Universiti Putra Malaysia, 43400 UPM Serdang, Selangor, Malaysia; E-Mail:
Int J Mol Sci. 2010 Oct 12;11(10):3898-905. doi: 10.3390/ijms11103898.
Silver nanoparticles (Ag-NPs) were successfully synthesized in the natural polymeric matrix. Silver nitrate, gelatin, glucose, and sodium hydroxide have been used as silver precursor, stabilizer, reducing agent, and accelerator reagent, respectively. This study investigated the role of NaOH as the accelerator. The resultant products have been confirmed to be Ag-NPs using powder X-ray diffraction (PXRD), UV-vis spectroscopy, and transmission electron microscopy (TEM). The colloidal sols of Ag-NPs obtained at different volumes of NaOH show strong and different surface plasmon resonance (SPR) peaks, which can be explained from the TEM images of Ag-NPs and their particle size distribution. Compared with other synthetic methods, this work is green, rapid, and simple to use. The newly prepared Ag-NPs may have many potential applications in chemical and biological industries.
成功地在天然聚合基质中合成了银纳米粒子(Ag-NPs)。硝酸银、明胶、葡萄糖和氢氧化钠分别用作银前体、稳定剂、还原剂和加速剂试剂。本研究探讨了 NaOH 作为加速剂的作用。使用粉末 X 射线衍射 (PXRD)、紫外-可见光谱和透射电子显微镜 (TEM) 证实了所得产物为 Ag-NPs。在不同体积的 NaOH 条件下获得的 Ag-NPs 胶体溶胶显示出强且不同的表面等离子体共振 (SPR) 峰,可以从 Ag-NPs 的 TEM 图像及其粒径分布来解释。与其他合成方法相比,这项工作绿色、快速且易于使用。新制备的 Ag-NPs 在化学和生物工业中可能具有许多潜在的应用。