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预热型复合材料的颜色稳定性、不透明度和转化率。

Color stability, opacity and degree of conversion of pre-heated composites.

机构信息

Department of Dental Materials and Prosthodontics, Ribeirão Preto School of Dentistry, University of São Paulo, Ribeirão Preto, SP, Brazil.

出版信息

J Dent. 2011 Jul;39 Suppl 1:e25-9. doi: 10.1016/j.jdent.2010.12.001. Epub 2010 Dec 14.

Abstract

OBJECTIVES

To assess color stability and opacity associated with the degree of conversion of a pre-heated nanohybrid composite (Tetric N-Ceram, Ivoclar/Vivadent, Schaan, Liechtenstein).

METHODS

Twenty-seven specimens were prepared (n=9) using a Teflon matrix following storage of compules containing the composite at temperatures of 8°C, 25°C or 60°C. After photoactivation and polishing, baseline readings of six specimens were taken regarding their color and opacity (Spectrophotometer PCB 6807, Byk Gardner, Geretsried, Germany). Then, the specimens were submitted to artificial ageing for 384 h (C-UV, Adexim Comexim, São Paulo, SP, Brazil), after which the final readings were taken. Three specimens for each temperature were submitted to analysis of degree of conversion (Nicolet 380, Thermo Scientific, Waltham, MA, USA). The results were analysed by 1-way ANOVA/Tukey (p<0.05).

RESULTS

There was no significant difference in color stability and opacity variation amongst the temperatures evaluated. The composite pre-heated at 60°C had a higher degree of conversion (65.13%), with statistically significant difference compared to the other temperatures (p<0.05).

CONCLUSIONS

Composite pre-heating does not promote changes in the optical properties, despite the increase in the degree of conversion.

摘要

目的

评估加热纳米复合树脂(Tetric N-Ceram,义获嘉伟瓦登特,列支敦士登)的转化率与其颜色稳定性和不透明度的关系。

方法

使用聚四氟乙烯基质制备了 27 个样本(n=9),在将包含复合材料的压缩块储存在 8°C、25°C 或 60°C 的温度下。光固化和抛光后,对 6 个样本的颜色和不透明度进行了基线读数(Byk Gardner,德国 Geretsried 的 Spectrophotometer PCB 6807)。然后,将样本进行 384 小时的人工老化(巴西 São Paulo 的 C-UV,Adexim Comexim),之后进行最终读数。对每个温度的 3 个样本进行转化率分析(Thermo Scientific,美国马萨诸塞州 Waltham 的 Nicolet 380)。结果采用单因素方差分析/Tukey 检验(p<0.05)。

结果

在所评估的温度下,颜色稳定性和不透明度变化无显著差异。与其他温度相比,加热至 60°C 的复合材料转化率(65.13%)更高,差异有统计学意义(p<0.05)。

结论

尽管转化率增加,但复合材料的预加热不会导致光学性能发生变化。

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