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现代复合材料在不同加速人工老化周期下的颜色稳定性。

Color stability of modern composites subjected to different periods of accelerated artificial aging.

作者信息

Drubi-Filho Brahim, Garcia Lucas da Fonseca Roberti, Cruvinel Diogo Rodrigues, Sousa Ana Beatriz Silva, Pires-de-Souza Fernanda de Carvalho Panzeri

机构信息

Department of Dental Materials and Prosthodontics, Ribeirão Preto Dental School, University of São Paulo, Brazil.

出版信息

Braz Dent J. 2012;23(5):575-80. doi: 10.1590/s0103-64402012000500018.

Abstract

The aim of this study was to evaluate the color stability of composites subjected to different periods of accelerated artificial aging (AAA). A polytetrafluorethylene matrix (10 x 2 mm) was used to fabricate 24 test specimens of three different composites (n=8): Tetric Ceram (Ivoclar/Vivadent); Filtek P90 and Z250 (3M ESPE), shade A3. After light activation for 20 s (FlashLite 1401), polishing and initial color readout (Spectrophotometer PCB 687; BYK Gardner), the test specimens were subjected to AAA (C-UV; Comexim), in 8-h cycles: 4 h exposure to UV-B rays at 50°C and 4 h condensation at 50°C. At the end of each cycle, color readouts were taken and the test ended when the mean value of ΔE attained a level ≥3.30. Tetric Ceram presented alteration in ΔE equal to 3.33 in the first aging cycle. For Filtek P90 and Z250, two (ΔE=3.60) and four (ΔE=3.42) AAA cycles were necessary. After each cycle, there was a reduction of luminosity in all the samples (ΔL). It was concluded that a short period of AAA was sufficient to promote clinically unacceptable color alteration in composites, and that this alteration was material-dependent.

摘要

本研究的目的是评估经受不同时间段加速人工老化(AAA)的复合材料的颜色稳定性。使用聚四氟乙烯基质(10×2毫米)制作三种不同复合材料(n = 8)的24个测试样本:Tetric Ceram(义获嘉伟瓦登特公司);Filtek P90和Z250(3M公司),色号A3。在光固化20秒(FlashLite 1401)、抛光并进行初始颜色读数(分光光度计PCB 687;BYK Gardner)后,测试样本接受AAA(C - UV;Comexim公司),以8小时为周期:在50°C下暴露于UV - B射线4小时,在50°C下冷凝4小时。在每个周期结束时进行颜色读数,当ΔE的平均值达到≥3.30的水平时测试结束。Tetric Ceram在第一个老化周期中ΔE的变化等于3.33。对于Filtek P90和Z250,分别需要两个(ΔE = 3.60)和四个(ΔE = 3.42)AAA周期。在每个周期后,所有样本的亮度均有所降低(ΔL)。得出的结论是,短时间的AAA足以促进复合材料出现临床上不可接受的颜色变化,并且这种变化取决于材料。

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