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Diaqua-(2,5-di-4-pyridyl-1,3,4-thia-diazole-κN)bis-(thio-cyanato-κN)nickel(II) dihydrate.

作者信息

Yang Ming-Hua

机构信息

Department of Chemistry, Lishui University, Lishui 323000, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Sep 27;64(Pt 10):m1331. doi: 10.1107/S1600536808030444.

DOI:10.1107/S1600536808030444
PMID:21201065
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2959476/
Abstract

In the title mononuclear complex, [Ni(NCS)(2)(C(12)H(8)N(4)S)(2)(H(2)O)(2)]·2H(2)O, the Ni(II) atom is located on an inversion center and is octa-hedrally coordinated by four N atoms from two 2,5-di-4-pyridyl-1,3,4-thia-diazole (bpt) ligands and two thio-cyanate mol-ecules forming the equatorial plane; the axial positions are occupied by two O atoms of coordinated water mol-ecules. O-H⋯O, O-H⋯N and O-H⋯S hydrogen bonds, involving the uncoordinated water molecules, result in the formation of a sheet structure developing parallel to (021).

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1f6d/2959476/66a20651e6d6/e-64-m1331-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1f6d/2959476/aed2570cfa46/e-64-m1331-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1f6d/2959476/66a20651e6d6/e-64-m1331-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1f6d/2959476/aed2570cfa46/e-64-m1331-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1f6d/2959476/66a20651e6d6/e-64-m1331-fig2.jpg

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本文引用的文献

1
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Acta Crystallogr Sect E Struct Rep Online. 2008 Apr 10;64(Pt 5):m630. doi: 10.1107/S1600536808008854.
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A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
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Self-assembly of coordination polymers from AgX (X = SbF(6)(-), PF(6)(-), and CF(3)SO(3)(-)) and oxadiazole-containing ligands.
由AgX（X = SbF₆⁻、PF₆⁻和CF₃SO₃⁻）与含恶二唑配体自组装形成配位聚合物。
Inorg Chem. 2003 Sep 8;42(18):5699-706. doi: 10.1021/ic034306t.
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First Cu(II) diamondoid net with 2-fold interpenetrating frameworks. The role of anions in the construction of the supramolecular arrays.
Inorg Chem. 2002 Sep 23;41(19):4904-8. doi: 10.1021/ic025559+.