二甲基[1-(1-烯丙基-5-碘-1H-吲哚-3-基)-3-羟基丙基]膦酸酯
Dimethyl [1-(1-allyl-5-iodo-1H-indol-3-yl)-3-hydroxy-prop-yl]phospho-nate.
作者信息
Guo Ying-Cen, Wang Xu-Fan, Ding Yu
机构信息
Key Laboratory of Pesticides and Chemical Biology of Ministry of Education, College of Chemistry, Central China Normal University, Wuhan 430079, People's Republic of China.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2008 Jan 9;64(Pt 2):o384. doi: 10.1107/S1600536807068171.
Abstract
In the title compound, C(16)H(21)INO(4)P, the mol-ecular structure is stabilized by a weak intra-molecular C-H⋯O hydrogen-bond inter-action. The crystal packing is stabilized by strong inter-molecular O-H ⋯ O hydogen-bonding inter-actions to form a zigzag packing arrangement.
摘要
在标题化合物C₁₆H₂₁INO₄P中，分子结构通过弱的分子内C-H⋯O氢键相互作用得以稳定。晶体堆积通过强的分子间O-H⋯O氢键相互作用得以稳定，从而形成一种锯齿状堆积排列。
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本文引用的文献
1
A short history of SHELX.
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
2
Catalytic enantioselective Friedel-Crafts alkylations of indoles with alpha'-phosphoric enones.
Org Lett. 2007 Jun 7;9(12):2281-4. doi: 10.1021/ol070548b. Epub 2007 May 11.
3
Enantioselective organocatalytic hydrophosphination of alpha,beta-unsaturated aldehydes.
Angew Chem Int Ed Engl. 2007;46(24):4507-10. doi: 10.1002/anie.200700916.
4
Organocatalytic asymmetric hydrophosphination of alpha,beta-unsaturated aldehydes.
Angew Chem Int Ed Engl. 2007;46(24):4504-6. doi: 10.1002/anie.200700754.
5
1-(1H-Indol-3-ylcarbonyl)-N-(4-methoxybenzyl)formamide.
Acta Crystallogr C. 2006 Mar;62(Pt 3):o153-4. doi: 10.1107/S0108270106003441. Epub 2006 Feb 28.
6
Isolation of 2-aminoethane phosphonic acid from rumen protozoa.
Nature. 1959 Sep 19;184(Suppl 12):901-2. doi: 10.1038/184901b0.
7
Renin inhibitors. Synthesis of transition-state analogue inhibitors containing phosphorus acid derivatives at the scissile bond.
J Med Chem. 1989 Jul;32(7):1652-61. doi: 10.1021/jm00127a041.
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