N'-(4-甲氧基-亚苄基)-4-硝基-苯甲酰肼甲醇溶剂合物
N'-(4-Methoxy-benzyl-idene)-4-nitro-benzo-hydrazide methanol solvate.
作者信息
Wang Yuan-Zhi, Wang Ming-Dong, Diao Yun-Peng, Cai Qian
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2008 Mar 5;64(Pt 4):o668. doi: 10.1107/S1600536808005813.
Abstract
The title compound, C(15)H(13)N(3)O(4)·CH(4)O, was synthesized from the reaction of 4-methoxy-benzaldehyde with 4-nitro-benzohydrazide in methanol. The benzene rings of the Schiff base mol-ecule are nearly coplanar, making a dihedral angle of 7.0 (3)°. The methanol solvent mol-ecules are linked to the Schiff base mol-ecules by N-H⋯O, O-H⋯N and O-H⋯O hydrogen bonds, forming chains running parallel to the b axis.
摘要
标题化合物C(15)H(13)N(3)O(4)·CH(4)O是由4-甲氧基苯甲醛与4-硝基苯甲酰肼在甲醇中反应合成的。席夫碱分子的苯环几乎共面，二面角为7.0 (3)°。甲醇溶剂分子通过N-H⋯O、O-H⋯N和O-H⋯O氢键与席夫碱分子相连，形成平行于b轴的链。
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