（E）-3-溴-N'-（4-甲氧基-亚苄基）苯甲酰肼甲醇溶剂化物
(E)-3-Bromo-N'-(4-methoxy-benzyl-idene)benzohydrazide methanol solvate.
作者信息
Cao Guo-Biao
机构信息
Department of Chemistry, Ankang University, Ankang Shanxi 725000, People's Republic of China.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2009 Aug 8;65(Pt 9):o2086. doi: 10.1107/S1600536809030219.
The title compound, C(15)H(13)BrN(2)O(2)·CH(3)OH, was synthesized by the reaction of 4-methoxy-benzaldehyde with an equimolar quantity of 3-bromo-benzohydrazide in methanol. The benzohydrazide mol-ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 4.0 (2)°. The benzohydrazide and methanol mol-ecules are linked into a chain propagating along the b axis by O-H⋯O, O-H⋯N, N-H⋯O and C-H⋯O hydrogen bonds.
标题化合物C(15)H(13)BrN(2)O(2)·CH(3)OH是由4-甲氧基苯甲醛与等摩尔量的3-溴苯甲酰肼在甲醇中反应合成的。苯甲酰肼分子围绕C=N键呈E构型。两个苯环之间的二面角为4.0 (2)°。苯甲酰肼和甲醇分子通过O-H⋯O、O-H⋯N、N-H⋯O和C-H⋯O氢键连接成沿b轴延伸的链。
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