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N'-(2-羟基-亚苄基)-4-甲氧基-苯甲酰肼

N'-(2-Hydroxy-benzyl-idene)-4-methoxy-benzohydrazide.

作者信息

Tang Chun-Bao

机构信息

Department of Chemistry, Jiaying University, Meizhou 514015, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Mar 29;64(Pt 4):o767. doi: 10.1107/S1600536808008088.

DOI:10.1107/S1600536808008088
PMID:21202154
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2961042/
Abstract

The title Schiff base compound, C(15)H(14)N(2)O(3), was derived from the condensation reaction of salicylaldehyde with 4-methoxy-benzohydrazide. The dihedral angle between the two benzene rings is 2.5 (2)°. In the crystal structure, mol-ecules are linked through inter-molecular N-H⋯O hydrogen bonds, forming chains running along the b axis.

摘要

席夫碱化合物C(15)H(14)N(2)O(3)由水杨醛与4-甲氧基苯甲酰肼缩合反应得到。两个苯环之间的二面角为2.5 (2)°。在晶体结构中，分子通过分子间N-H⋯O氢键相连，形成沿b轴延伸的链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/393e/2961042/44d8cdb63529/e-64-0o767-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/393e/2961042/1067e99fc4a4/e-64-0o767-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/393e/2961042/44d8cdb63529/e-64-0o767-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/393e/2961042/1067e99fc4a4/e-64-0o767-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/393e/2961042/44d8cdb63529/e-64-0o767-fig2.jpg

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本文引用的文献

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A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.