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N'-(2-羟基-亚苄基)-2-甲氧基苯甲酰肼一水合物

N'-(2-Hydroxy-benzyl-idene)-2-methoxy-benzohydrazide monohydrate.

作者信息

Lu Jiu-Fu, Min Suo-Tian, Ji Xiao-Hui, Dang Zhong-Hai

机构信息

School of Chemistry and Environmental Science, Shaanxi University of Technology, Hanzhong 723000, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Aug 6;64(Pt 9):o1693. doi: 10.1107/S1600536808024483.

DOI:10.1107/S1600536808024483
PMID:21201682
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2960617/
Abstract

In the title compound, C(15)H(14)N(2)O(3)·H(2)O, the Schiff base mol-ecule is approximately planar, with a dihedral angle between the two aromatic rings of 10.2 (3)°. The mol-ecular structure is stabilized by O-H⋯N and N-H⋯O hydrogen bonds. In the crystal structure, the Schiff base and water mol-ecules are linked together by inter-molecular O-H⋯O hydrogen bonds, forming chains parallel to the a axis.

摘要

在标题化合物C₁₅H₁₄N₂O₃·H₂O中，席夫碱分子近似呈平面状，两个芳环之间的二面角为10.2 (3)°。分子结构通过O—H⋯N和N—H⋯O氢键得以稳定。在晶体结构中，席夫碱和水分子通过分子间O—H⋯O氢键连接在一起，形成平行于a轴的链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3580/2960617/b6364f6c36e4/e-64-o1693-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3580/2960617/0601bfa469f1/e-64-o1693-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3580/2960617/b6364f6c36e4/e-64-o1693-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3580/2960617/0601bfa469f1/e-64-o1693-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3580/2960617/b6364f6c36e4/e-64-o1693-fig2.jpg

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