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N'-(2-羟基萘基亚甲基)-4-甲氧基苯甲酰肼

N'-(2-Hydroxy-naphthyl-idene)-4-methoxy-benzo-hydrazide.

作者信息

Tang Chun-Bao

机构信息

Department of Chemistry, Jiaying University, Meizhou 514015, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Mar 29;64(Pt 4):o768. doi: 10.1107/S1600536808008076.

DOI:10.1107/S1600536808008076
PMID:21202155
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2960934/
Abstract

The title Schiff base compound, C(19)H(16)N(2)O(3), was derived from the condensation reaction of 2-hydr-oxy-1-naphthyl-aldehyde with 4-methoxy-benzohydrazide. The dihedral angle between the benzene ring and the naphthyl ring system is 6.8 (2)°. In the crystal structure, mol-ecules are linked through inter-molecular N-H⋯O inter-molecular hydrogen bonds, forming chains running along the c axis.

摘要

席夫碱化合物C(19)H(16)N(2)O(3)由2-羟基-1-萘甲醛与4-甲氧基苯甲酰肼缩合反应得到。苯环与萘环系统之间的二面角为6.8 (2)°。在晶体结构中，分子通过分子间N-H⋯O分子间氢键相连，形成沿c轴延伸的链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/55e0/2960934/a7492100b0c8/e-64-0o768-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/55e0/2960934/2e4bdeb909de/e-64-0o768-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/55e0/2960934/a7492100b0c8/e-64-0o768-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/55e0/2960934/2e4bdeb909de/e-64-0o768-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/55e0/2960934/a7492100b0c8/e-64-0o768-fig2.jpg

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A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.