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1,2-双[(2-羟基-3-甲氧基-亚苄基)腙基]-1,2-二苯基乙烷

1,2-Bis[(2-hydr-oxy-3-methoxy-benzyl-idene)hydrazono]-1,2-diphenyl-ethane.

作者信息

Zhang Xiu-Ying, Ma Hui, Chang Jiu-Li, Wu Xin-Cheng

机构信息

Henan Normal University, College of Chemistry and Environmental Science, Xinxiang 453002, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 May 17;64(Pt 6):o1090. doi: 10.1107/S1600536808014049.

DOI:10.1107/S1600536808014049
PMID:21202605
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2961346/
Abstract

The title compound, C(30)H(26)N(4)O(4), was synthesized by the reaction of benzyl dihydrazone and 2-hydr-oxy-3-methoxy-benzaldehyde in ethanol. In the crystal strucutre, the mol-ecule is centrosymmetric. The structure displays two symmetry-related intra-molecular O-H⋯N hydrogen bonds.

摘要

标题化合物C(30)H(26)N(4)O(4)是通过苄基二腙与2-羟基-3-甲氧基苯甲醛在乙醇中反应合成的。在晶体结构中，分子是中心对称的。该结构显示出两个与对称相关的分子内O-H⋯N氢键。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9fb/2961346/5d2733fc6fc9/e-64-o1090-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9fb/2961346/5d2733fc6fc9/e-64-o1090-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c9fb/2961346/5d2733fc6fc9/e-64-o1090-fig1.jpg

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本文引用的文献

1
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
2
New poly-iron(II) complexes of N4O dinucleating Schiff bases and pseudohalides: syntheses, structures, and magnetic and Mössbauer properties.新型N4O双核席夫碱与拟卤化物的聚铁（II）配合物：合成、结构以及磁学和穆斯堡尔性质
Inorg Chem. 2004 Feb 23;43(4):1574-86. doi: 10.1021/ic0351904.
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Calix[4]pyrrole Schiff base macrocycles. Novel binucleating ligands for mu-oxo iron complexes.杯[4]吡咯席夫碱大环化合物。用于μ-氧代铁配合物的新型双核配体。
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