Rodziewicz Lech, Zawadzka Iwona
Zakad Higieny Weterynaryjnej, Wojewódzki Inspektorat Weterynarii, Białystok.
Rocz Panstw Zakl Hig. 2010;61(3):249-52.
The method is presented to analyze chloramphenicol in milk powder. Sample was clean-up by used molecular imprinted polymers (MIP). The determination was performed by LC-ESI-MS/MS. The LC was equipped with column Luna C18 Phenomenex. CAP-d5 was used as internal standards. The method was validation according to the criteria of Decision Commission No 2002/657/EC. Recoveries for the level 0.3 microg/kg was in the range 104-111%. The limit of decision (CCalpha) and detection capability (CCbeta) was respectively 0.06 microg/kg and 0.09 microg/kg.
介绍了分析奶粉中氯霉素的方法。样品通过使用分子印迹聚合物（MIP）进行净化。采用LC-ESI-MS/MS进行测定。液相色谱配备Phenomenex Luna C18柱。CAP-d5用作内标。该方法根据欧盟委员会第2002/657/EC号决定的标准进行验证。0.3微克/千克水平的回收率在104-111%范围内。决策限（CCalpha）和检测能力（CCbeta）分别为0.06微克/千克和0.09微克/千克。
