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[Quantitative determination of strychnine in blood and urine by gas chromatography with mass-selective detector].

作者信息

Kataev S S, Krylova E A

出版信息

Sud Med Ekspert. 2010 Nov-Dec;53(6):35-8.

PMID:21404532
Abstract

A method for the quantitative determination of strychnine in biological fluids by gas chromatography--mass spectrometry is proposed. The preparation of samples for the analysis included extraction of strychnine from blood and urine with the use of AccuBond(II) EVIDEX cartridges for solid-phase extraction and SPEC MP3 disks respectively. The efficiency of extraction was estimated at 0.05 mg/l for blood and 0.02 mg/l for urine. The detection limit was 0.10 mg/l in blood and 0.05 mg/l in urine.

摘要

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