Dehestru Guillaume, Leman Marie, Jundt Jacques, Dryden Phil, Sullivan Matthew, Harrison Christopher
Schlumberger-Doll Research, 1 Hampshire Street, Cambridge, Massachusetts 02139, USA.
Rev Sci Instrum. 2011 Mar;82(3):035113. doi: 10.1063/1.3563721.
This article discusses a microfluidic vibrating wire viscometer with an internal volume of a few microliters. Accuracy of order ±10% for viscosities ranging from 0.1 to 100 cP is demonstrated for temperatures (10 °C-175 °C) and pressures (10-24,000 psi) suitable for oilfield use by prior calibration in air and toluene. Comparison between multiple data sets indicates that a large fraction of the discrepancy between literature values is systematic, indicating that future refinements may be possible with better interpretation. Confinement effects are evaluated and are not found to play a significant role, which is surprising since the ratio (6.6) of the fluid channel width to the wire diameter is very low.
本文讨论了一种内部容积为几微升的微流控振弦粘度计。通过在空气和甲苯中进行预先校准,在适用于油田使用的温度(10℃至175℃)和压力(10至24,000 psi)下,对于0.1至100 cP的粘度,展示了±10%左右的精度。多个数据集之间的比较表明,文献值之间的很大一部分差异是系统性的,这表明通过更好的解释未来可能进行改进。对限制效应进行了评估,发现其并未发挥显著作用,这令人惊讶,因为流体通道宽度与金属丝直径之比(6.6)非常低。